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Title: Synthesis of pyrimidinocyclophanes having a bridging nitrogen atom.
Authors: Semenov, V. E.; Nikolaev, A. E.; Kozlov, A. V.; Efremov, Yu. Ya.; Latypov, Sh. K.; Reznik, V. S.
Abstract: Reactions of 1,3-bis(ω-bromoalkyl)-substituted uracils, quinazoline-2,4-dione, and 5-methyl-1,3,5-triazine-2,4,6-trione and 1,3-bis( m-bromomethylbenzyl)-5-bromouracil with amines (aliphatic amines, benzylamines, naphthylmethanamine, and anisidine) gave a series of macrocyclic compounds having one pyrimidine or triazine fragment and an azapolymethylene bridge connecting the N1 and N3 atoms of the heteroring. The bridging nitrogen atom in some macrocyclic compounds was subjected to quaternization with methyl p-toluenesulfonate.
Subjects: NITROGEN; CHEMICAL reactions; URACIL; TRIAZINES; ORGANIC compounds; MACROCYCLIC compounds
Publication: Russian Journal of Organic Chemistry, 2008, Vol 44, Issue 6, p882
ISSN: 1070-4280
Publication type: Academic Journal
DOI: 10.1134/S1070428008060183

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Synthesis of pyrimidinocyclophanes having a bridging nitrogen atom.