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- Title
Selective acetylation of primary amino groups with phenyl acetate: simple conversion of polyamines into N,N'-diacetyl derivatives.
- Authors
Ucal, Sebahat; Khomutov, Alex R.; Häkkinen, Merja R.; Turhanen, Petri A.; Vepsäläinen, Jouko J.; Weisell, Janne
- Abstract
Phenyl acetate was studied as a general reagent for highly selective N-acetylation of primary amino groups in the presence of alcohol and secondary amino groups. Two polyamines, namely 1,8-diamino-4-azaoctane (Spd) and 1,12-diamino-4,9-diazadodecane (Spm), were N,N'-diacetylated with an efficient and mild methodology.
- Subjects
PHENYLACETATES; ACETYLATION; AMINO group; ALCOHOL; POLYAMINES
- Publication
ARKIVOC: Online Journal of Organic Chemistry, 2015, Vol 2015, p42
- ISSN
1551-7004
- Publication type
Academic Journal
- DOI
10.3998/ark.5550190.p009.169