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Title

Four-Component Synthesis of 9 H -Pyrimido[4,5- b ]indoles Using Ammonium Iodide as the Nitrogen Source.

Authors

Chen, Yufeng; Yang, Ruitong; Xiao, Fuhong; Li, Tong; Mao, Guojiang; Deng, Guo-Jun

Abstract

A four-component synthesis of 2-phenyl-9H-pyrimido[4,5-b]indoles was developed using indole-3-carboxaldehydes, aromatic aldehyde and ammonium iodide as the raw materials under transition-metal-free conditions. The pyrimidine ring was formed in one pot through [4 2] annulation reaction. Four C–N bonds were formed in one pot promoted by iodine and iodide additives. This work is highlighted by using two ammonium iodides as the sole nitrogen source.

Subjects

INDOLE compounds; INDOLE; IODIDES; AROMATIC aldehydes; AMMONIUM; NITROGEN

Publication

Catalysts (2073-4344), 2023, Vol 13, Issue 3, p623

ISSN

2073-4344

Publication type

Academic Journal

DOI

10.3390/catal13030623

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