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- Title
POTENTIAL PROCESS RELATED SUBSTANCE OF ATORVASTATIN CALCIUM: IDENTIFICATION, SYNTHESIS AND SPECTRAL CHARACTERIZATION INCLUDING CONTROL STRATEGY.
- Authors
Gutta, Madhusudhan; Chakradhar, Nandigama; Kotte, Chandramohan; Kokkula, Kishore; Mittapelli, Vasantha
- Abstract
HPLC analysis of Atorvastatin Calcium showed an unknown compound peak, the sample was also analyzed by LCMS and the corresponding peak was identified at m/z 854.06. The pure compound was prepared individually and characterized. The compound structure was assigned as tert-butyl 2-((4R,6R)-6-(2-(2-((4R,6R)-6-(2-[2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-phenylcarbamoyl-pyrrol-1-yl]-ethyl)-2,2-dimethyl-1,3-dioxan-4- yl)acetamido)ethyl)-2,2-dimethyl-1,3-dioxan-4-yl)acetate.
- Subjects
ATORVASTATIN; CALCIUM; HIGH performance liquid chromatography; CONDENSATION; ACETATES
- Publication
Rasayan Journal of Chemistry, 2024, Vol 17, Issue 4, p1573
- ISSN
0974-1496
- Publication type
Academic Journal
- DOI
10.31788/RJC.2024.1748984