Title: Synthesis of β-enaminoesters from β-ketoesters and amines by solvent-drop grinding approach in PEG 400.
Authors: Mukhedkar, Swanand S.; Digambar, Kokane Balaji; Deshmukh, Jitendra Hanmantrao; Anjanikar, Shivraj Shankarrao
Abstract: An effective catalytic system for the synthesis of ß-enaminoesters from ß-ketoesters under mechanochemical conditions using mortar and pestle in recyclable PEG 400 as solvent-drop approach was developed. This method has a number of benefits, including shorter reaction times, use of inexpensive recyclable solvent cum catalyst system, compatible reaction conditions, and high product yields. ©2024 ACG Publications. All rights reserved.
Subjects: POLYETHYLENE glycol; CATALYSIS; CATALYSTS; AMINES; SOLVENTS
Publication: Organic Communications, 2024, Vol 17, Issue 4, p241
ISSN: 1307-6175
Publication type: Academic Journal
DOI: 10.25135/acg.oc.178.2409.3334

Synthesis of β-enaminoesters from β-ketoesters and amines by solvent-drop grinding approach in PEG 400.

Mukhedkar, Swanand S.; Digambar, Kokane Balaji; Deshmukh, Jitendra Hanmantrao; Anjanikar, Shivraj Shankarrao