This work aims to test the use of scales from the cones of the Araucaria angusti-folia tree in the removal of chromium and iron encountered in the wastewaters from the galvanoplasty process. A comparison with other treatment methods was also per-formed for compliance with environmental legislation. The cone scales are obtained from "pinhão", which is consumed in the south Brazil. Some parameters were opti-mized for the best performance of metal removal, such as biosorbent particles size and dosage, pH, time of contact and initial metal concentrations. The results were com-pared with adsorption treatment using activated carbon and chemical precipitation with bisulfite. The cone scales are efficient for the removal of chromium(VI) (> 99%), while the iron concentration was 62% lower after 1 hour of the contact with 3 g.L1 of the sorbent (particle size <250 fim). The scales showed to be competitive with the tra-ditional processes, allowing also a more noble use a material that would be discarded.