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Title

Potentialities of Reaction Sintering in the Fabrication of High-Strength Macroporous Ceramics Based on Substituted Calcium Phosphate.

Authors

Orlov, N. K.; Kiseleva, A. K.; Milkin, P. A.; Evdokimov, P. V.; Putlayev, V. I.; Günster, J.

Abstract

Calcium alkali metal (potassium and sodium) double and triple phosphates have been synthesized in different ways. Was for the first time used reaction sintering to produce ceramics based on calcium alkali metal mixed phosphates and investigated the densification behavior of mixed phosphate-based multiphase materials during sintering by this method. Was presented the microstructure of polished surfaces of sintered samples differing in phase composition and determined the density of ceramics prepared using reaction mixtures differing in composition. The effect of reaction sintering on the porosity of the ceramics has been assessed. Using stereolithographic printing and reaction sintering, was produced macroporous mixed calcium phosphate-based ceramic implants. Their compressive strength has been determined to be 0.78 ± 0.21 MPa for two-phase samples and 1.02 ± 0.13 MPa for three-phase samples.

Subjects

CALCIUM phosphate; COMPOSITE materials; ALKALI metals; SINTERING; CERAMICS; STEREOLITHOGRAPHY; MICROWAVE sintering

Publication

Inorganic Materials, 2020, Vol 56, Issue 12, p1298

ISSN

0020-1685

Publication type

Academic Journal

DOI

10.1134/S0020168520120146

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