Title: Growth and characterization of tris thiourea chromium(III) sulphate.
Authors: Madhurambal, G.; Ravindran, B.; Mariappan, M.; Mojumdar, S.
Abstract: Single crystal of tris thiourea chromium(III) sulphate was grown by slow evaporation technique at 303 K. The structural properties of the grown crystals were characterized by FTIR spectroscopy, UV spectroscopy and powder X-ray diffraction analysis. FTIR and UV spectra provide information about the presence of functional groups. Thermal analysis confirms that the crystal is thermally stable up to 163.48 °C. The TG curve presented a two-step mass loss on heating the compound at 0-1,200 °C.
Subjects: THIOUREA; CHROMIUM sulfide; SINGLE crystals; CHEMICAL structure; FOURIER transform infrared spectroscopy; FUNCTIONAL groups; EVAPORATION (Chemistry)
Publication: Journal of Thermal Analysis & Calorimetry, 2012, Vol 108, Issue 3, p905
ISSN: 1388-6150
Publication type: Academic Journal
DOI: 10.1007/s10973-012-2360-0

Growth and characterization of tris thiourea chromium(III) sulphate.

Madhurambal, G.; Ravindran, B.; Mariappan, M.; Mojumdar, S.