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- Title
Electrochemical Determination of Triclosan Using ZIF-11/Activated Carbon Derived from the Rice Husk Modified Electrode.
- Authors
Luyen, Nguyen Dinh; Toan, Tran Thanh Tam; Trang, Ha Thuy; Nguyen, Vo Thang; Son, Le Van Thanh; Thanh, Tran Si; Thanh, Nguyen Mau; Quy, Phan Tu; Khieu, Dinh Quang
- Abstract
In the present paper, the composite of zeolite imidazolate framework-11 (ZIF-11) and activated carbon derived from rice husks (RHAC) was synthesized. The obtained materials were characterized by XRD, SEM, EDX-mapping, and nitrogen adsorption/desorption isotherms. The final composite ZIF-11/RHAC exhibits an even dispersion of ZIF-11 particles on activated carbon matrix. Herein, an electrochemical sensor based on a ZIF-11/RHAC was developed for a rapid determination of triclosan (TCS). It was found that the oxidation of TCS is irreversible and involves the transfer of one electron. The linear range for TCS detection in the optimized experimental conditions was found to be 0.1-8 μM with the limit of detection of 0.076 μM. Finally, the proposed method was successfully employed to detect TCS in different personal care product samples with high accuracy, which was confirmed by a good agreement between these results and those obtained using high-performance liquid chromatography (HPLC).
- Subjects
RICE hulls; ACTIVATED carbon; TRICLOSAN; HIGH performance liquid chromatography; ELECTROCHEMICAL sensors; CHARGE exchange; HYGIENE products
- Publication
Journal of Nanomaterials, 2021, p1
- ISSN
1687-4110
- Publication type
Article
- DOI
10.1155/2021/8486962