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- Title
Synthesis of the First Dithiaaza-17-Crown-5 Ethers Containing Piperidin-4-One Subunit.
- Authors
Thi, Thanh Van Tran; Nguyen, Manh Linh; Nguyen, Tien Dat; Le, The Duan; Truong, Hong Hieu; Khrustalev, Victor N.; Le, Tuan Anh
- Abstract
Dithiaaza-17-crown-5 ethers containing piperidin-4-one subunit and dithiacrown ether fragment were synthesized in one-pot Petrenko–Kritschenko reaction from 2,2'-[ethane-1,2-diylbis(oxyethane-2,1-diylsulfanediyl)]dibenzaldehyde, methyl ethyl ketone or dibenzyl ketone, and ammonium acetate. Molecular structure of dithiaaza-17-crown-5 ethers were confirmed by NMR, HRMS, and single crystal X-ray diffraction.
- Subjects
AMMONIUM acetate; METHYL ethyl ketone; ETHERS; MOLECULAR structure; SINGLE crystals; X-ray diffraction
- Publication
Chemistry of Heterocyclic Compounds, 2021, Vol 57, Issue 10, p1057
- ISSN
0009-3122
- Publication type
Article
- DOI
10.1007/s10593-021-03022-1