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- Title
Scalable Flow Synthesis of [6,6]-Phenyl-C<sub>61</sub>-butyric Acid Methyl Ester (PCBM) using a Flow Photoreactor with a Sodium Lamp.
- Authors
Ueda, Mitsuhiro; Imai, Naoyuki; Yoshida, Shunsuke; Yasuda, Hiroshi; Fukuyama, Takahide; Ryu, Ilhyong
- Abstract
An efficient flow system was constructed for the synthesis of [6,6]-phenyl-C61-butyric acid methyl ester (PCBM); the process involved flow [2+1] addition of C60 and subsequent flow photoisomerization of the resulting fulleroid to PCBM by using a flow photoreactor in combination with an Na lamp. With the present flow system, a scalable synthesis of PCBM (0.79 g/3.3 h) was achieved by continuous operation for 3.3 h.
- Subjects
BUTYRIC acid; METHYL formate; PHENYL compounds; SODIUM; CHEMICAL reactors; CHEMICAL synthesis
- Publication
European Journal of Organic Chemistry, 2017, Vol 2017, Issue 44, p6483
- ISSN
1434-193X
- Publication type
Article
- DOI
10.1002/ejoc.201700745