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- Title
Magnetic Molecularly Imprinted Nano-Conjugates for Effective Extraction of Food Components—A Model Study of Tyramine Determination in Craft Beers.
- Authors
Luliński, Piotr; Janczura, Marta; Sobiech, Monika; Giebułtowicz, Joanna
- Abstract
In this paper, magnetic molecularly imprinted nano-conjugates were synthesized to serve as selective sorbents in a model study of tyramine determination in craft beer samples. The molecularly imprinted sorbent was characterized in terms of morphology, structure, and composition. The magnetic dispersive solid phase extraction protocol was developed and combined with liquid chromatography coupled with mass spectrometry to determine tyramine. Ten samples of craft beers were analyzed using a validated method, revealing tyramine concentrations in the range between 0.303 and 126.5 mg L−1. Tyramine limits of detection and quantification were 0.033 mg L−1 and 0.075 mg L−1, respectively. Therefore, the fabricated molecularly imprinted magnetic nano-conjugates with a fast magnetic responsivity and desirable adsorption performance could be an effective tool for monitoring tyramine levels in beverages.
- Subjects
TYRAMINE; CRAFT beer; LIQUID chromatography-mass spectrometry; SOLID phase extraction
- Publication
International Journal of Molecular Sciences, 2021, Vol 22, Issue 17, p9560
- ISSN
1661-6596
- Publication type
Article
- DOI
10.3390/ijms22179560