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- Title
Applications of sample-controlled thermal analysis (SCTA) to kinetic analysis and synthesis of materials.
- Authors
Pérez-Maqueda, L.; Criado, J.; Sánchez-Jiménez, P.; Diánez, M.
- Abstract
The advantages of the sample-controlled thermal analysis (SCTA) for both the kinetic analysis of solid-state reactions and the synthesis of materials are reviewed. This method implies an intelligent control of the temperature by the solid-state reaction under study in such a way that the reaction rate as a function of the time fits a profile previously defined by the user. It has been shown that SCTA has important advantages for discriminating the kinetic model of solid-state reactions as compared with conventional rising temperature methods. Moreover, the advantages of SCTA methods for synthesising materials with controlled texture and structure are analysed.
- Subjects
THERMAL analysis; CHEMICAL kinetics; CHEMICAL synthesis; SOLID state chemistry; CHEMICAL reactions
- Publication
Journal of Thermal Analysis & Calorimetry, 2015, Vol 120, Issue 1, p45
- ISSN
1388-6150
- Publication type
Article
- DOI
10.1007/s10973-014-4176-6