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- Title
Structure of a new chelate complex MOO(dpm).
- Authors
Ledneva, A.; Artemkina, S.; Stabnikov, P.; Yanshole, L.; Fedorov, V.
- Abstract
A new MoO(dpm) compound ( I) is synthesized by the interaction of Mo(CO) with 2,2,6,6-tetramethylheptanedione-3,5 (dpm). The structure of complex I determined by the XRD method is as follows: triclinic crystal system, space group P-1, a = 10.1780(7) Å, b = 10.1817(6) Å, c = 13.3255(9) Å, α = 110.562(2)°, β = 102.233(2)°, γ = 93.9041(19)°, V = 1248.17(14) Å. The compound is characterized by IR spectroscopy, mass-spectrometry and thermogravimetric analysis (TGA).
- Subjects
MOLYBDENUM; CHELATES; TRICLINIC crystal system; THERMOGRAVIMETRY; MASS spectrometry
- Publication
Journal of Structural Chemistry, 2017, Vol 58, Issue 4, p758
- ISSN
0022-4766
- Publication type
Article
- DOI
10.1134/S0022476617040163