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- Title
Three Cu(II) Complexes Constructed by Flexible bis-Imidazole and Different Anions: From 0D Architecture to 2D Layer.
- Authors
Lu, J. F.; Yu, X. H.; Zhao, C. B.; Zheng, N.; Yue, S. Y.; Li, L.; Tang, Z. H.; Ge, H. G.; Jin, L. X.
- Abstract
Three new Cu(II) complexes, Cu(1,3-bip)(Ac)2 (I), {[Cu(H2O)2(1,3-bip)2] · (NO3)2}n (II), {[Cu(1,3-bip)(1,4-bdc)]2 · H2O · MeOH}n (III), where 1,3-bip is 1,3-bis(imidazole)propane and 1,4-bdc is terephthalic acid, have been synthesized and characterized by single crystal and powder X-ray diffraction, Fourier transform infrared spectroscopy, and elemental analysis. Single crystal X-ray diffraction reveals that the complex I shows a zero-dimensional architecture, the complex II shows a one-dimensional loop-like chain, and the complex III shows a two-dimensional (4,4) grid layer structure. In addition, the thermal stability of complexes was investigated.
- Subjects
PHTHALIC acid; IMIDAZOLES; FOURIER transform infrared spectroscopy; X-ray powder diffraction; SINGLE crystals; ARCHITECTURE; TEREPHTHALIC acid
- Publication
Crystallography Reports, 2019, Vol 64, Issue 7, p1055
- ISSN
1063-7745
- Publication type
Article
- DOI
10.1134/S1063774519070095