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- Title
Synthesis, characterization, and crystal structure of bis[4-(3′-benzoyl)thiocarbamidophenyl]ether.
- Authors
Aydin, F.; Aykaç, D.; Burcu Arslan, N.; Kazak, C.
- Abstract
The title compound, bis[4-(3′-benzoyl)thiocarbamidophenyl]ether, was synthesized by the reaction of benzoylisothiocyanate with 4,4′-diaminodiphenylether in aprotic solvent. The structure was determinated by means of elemental analysis and FT-IR, H-NMR, 3C-NMR and MS spectroscopic techniques. The crystal structure was characterized by X-ray syngle crystal analysis: orthorhombic, sp. gr. Pnna, Z = 4. In crystal packing, there are intramolecular hydrogen bond N-H⋯O generating S(6) motif, and intermolecular hydrogen bond N-H⋯S forming R (8) ring.
- Subjects
THIOUREA; ISOTHIOCYANATES; CRYSTAL structure; ETHER synthesis; FOURIER transform infrared spectroscopy; SINGLE crystals; HYDROGEN bonding
- Publication
Crystallography Reports, 2014, Vol 59, Issue 7, p955
- ISSN
1063-7745
- Publication type
Article
- DOI
10.1134/S1063774514070050