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- Title
(25 S)-1α, 25, 26-Trihydroxycholecalciferol, a New Vitamin D<sub>3</sub> Metabolite: Synthesis and Absolute Stereochemistry at C(25).
- Authors
Partridge, John J.; Shiuey, Shian-Jan; Chadha, Naresh K.; Baggiolini, Enrico G.; Hennessy, Bernard M.; Uskoković, Milan R.; Napoli, Joseph L.; Reinhardt, Timothy A.; Horst, Ron L.
- Abstract
The 1α, 25, 26-trihydroxy metabolite of vitamin D3, isolated from bovine serum, was shown to possess the (25 S)-configuration by HPLC. comparison of the 1, 3, 26-triacetate derivative with authentic (25 R)- and (25 S)-samples. The convergent synthesis of (25 R)-1α, 25, 26- and (25 S)-1α, 25, 26-trihydroxycholecalciferols ( 10a) and ( 10b) has been accomplished.
- Publication
Helvetica Chimica Acta, 1981, Vol 64, Issue 7, p2138
- ISSN
0018-019X
- Publication type
Article
- DOI
10.1002/hlca.19810640718