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- Title
Crystal structure of pentafluoroacetanilide.
- Authors
Babailov, S.; Stabnikov, P.; Kuratieva, N.; Nikulshin, P.; Gromilov, S.
- Abstract
A new compound CFN(H)C(O)CH pentafluoroacetanilide, which is promising for the formation of coordination compounds with metal cations, is synthesized. Its crystal structure is determined (APEX DUO diffractometer, λMo K, graphite monochromator, T = 150 K). Crystallographic data for CHFNO are as follows: space group C2/ c, a = 18.2460(7) Å, b = 10.5840(4) Å, c = 9.4489(4) Å, β = 116.198(1)°, V = 1637.28(11) Å, Z = 8. The compound has a molecular structure formed of isolated pentafluoroacetanilide molecules. The average distances in the phenyl ring are 1.39 Å for C-C and 1.34 Å for C-F. The molecular structure of the studied compound is confirmed by F and H NMR in the solution CCl/CDCl = 1:1 (v:v).
- Subjects
POLYTYPIC transformations; CATIONIC lipids; NATIVE element minerals; DATA analysis; METAPHYSICS
- Publication
Journal of Structural Chemistry, 2015, Vol 56, Issue 6, p1201
- ISSN
0022-4766
- Publication type
Article
- DOI
10.1134/S002247661506030X