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- Title
Simplified Synthesis of Isotopically Labeled 5,5-Dimethyl-pyrroline N-Oxide.
- Authors
Leinisch, Fabian; JinJie Jiang; Deterding, Leesa J.; Mason, Ronald P.
- Abstract
5,5-Dimethylpyrroline N-oxide (15N) and 5,5-di(trideuteromethyl)pyrroline N-oxide were synthesized from the respective isotopically labeled 2-nitropropane analogs obtained from the reaction of sodium nitrate with 2-halopropanes. This facile, straightforward process allows synthesizing isotopically labeled DMPO analogs in a 4-step reaction without special equipment.
- Subjects
NITROPROPANE; SPIN trapping (Chemistry); CHEMICAL reagents; MASS spectrometry; ISOTOPES
- Publication
Molecules, 2011, Vol 16, Issue 10, p8428
- ISSN
1420-3049
- Publication type
Article
- DOI
10.3390/molecules16108428