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- Title
Aspects of the thermogravimetric analysis of liquid mixtures as predictive or interpretation tool for batch distillation.
- Authors
Tripodi, Antonio; Rossetti, Ilenia
- Abstract
The thermogravimetric analysis when applied to liquid binary mixtures of acetonitrile–water and methanol–water reproduces the whole course of a batch distillation with an appreciable saving of time and materials. The experimental mass and energy balances correlate with good approximation to the vapor–liquid equilibrium compositions without the need of gas-phase measures or thermodynamic models. This technique was here applied for the first time as fast method for distillation design and complementary tool for DSC boiling-point measurements.
- Subjects
THERMOGRAVIMETRY; LIQUID analysis; DISTILLATION; VAPOR-liquid equilibrium; BINARY mixtures; LIQUID mixtures
- Publication
Journal of Thermal Analysis & Calorimetry, 2022, Vol 147, Issue 12, p6765
- ISSN
1388-6150
- Publication type
Article
- DOI
10.1007/s10973-021-10990-1