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- Title
Reaction of 2,4-di- t-butyl-6-methylphenylphosphonous dichloride with chloroform in the presence of lithium diisopropylamide.
- Authors
Yoshifuji, Masaaki; Ito, Shigekazu; Toyota, Kozo; Yasunami, Masafumi
- Abstract
2,4-Di-t-butyl-6-methylphenylphosphonous dichloride reacted with chloroform in the presence of lithium diisopropylamide to give (2,4-di-t-butyl-6-methylphenyl) (dichloromethyl) (1,2,2-trichloroethenyl)phosphine. The structure of this phosphine was analyzed by X-ray crystallography. This phosphine further reacted with butyllithium to give (1-butylpentylidene)(2,4-di-t-butyl-6-methylphenyl)phosphine bearing a low-coordinated phosphorus atom. © 1996 John Wiley & Sons, Inc.
- Publication
Heteroatom Chemistry, 1996, Vol 7, Issue 1, p23
- ISSN
1042-7163
- Publication type
Article
- DOI
10.1002/(SICI)1098-1071(199601)7:1<23::AID-HC4>3.0.CO;2-3