We found a match
Your institution may have rights to this item. Sign in to continue.
- Title
The helical melamine-Keggin hybrid nanorods: syntheses and characterizations with two strategies, one-step solid-state chemical reaction and experimental solvent diffusion method.
- Authors
Farhadipour, Abolghasem; Eshghi, Hossein; Alizadeh, Mohammad; Yousefi, Mozhde; Artetxe, Beñat; Gutiérrez-Zorrilla, Juan
- Abstract
Two new Melamine-Keggin hybrid nanorods, MELH-PMo and MELH-PW, for the first time are successfully synthesized by two chemical methods, one-step solid-state chemical reaction method and experimental solvent diffusion method at room temperature. One-step solid-state reactions involve grounded nanorod materials along with grinding of row material and with solvent diffusion method these nanorods synthesized in single crystals form. These compounds crystallized in trigonal space groups P-3. Elemental analysis, infrared spectroscopy, UV spectroscopy and XRD analysis results prove that the samples still possess Keggin type structure. Transmittance electron microscopy and single-crystal X-ray have shown that the samples have nanorod structures.
- Subjects
MELAMINE; KEGGIN anions; NANORODS; SYNTHESIS of Nanocomposite materials; CHEMICAL reactions
- Publication
Journal of the Iranian Chemical Society, 2016, Vol 13, Issue 6, p1133
- ISSN
1735-207X
- Publication type
Article
- DOI
10.1007/s13738-016-0827-9