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- Title
A Facile Method for the Synthesis of Binary Tungsten Iodides.
- Authors
Ströbele, Markus; Castro, Cristina; Fink, Reinhold F.; Meyer, H.-Jürgen
- Abstract
The preparation of tungsten iodides in large quantities is a challenge because these compounds are not accessible using an easy synthesis method. A new, remarkably efficient route is based on a halide exchange reaction between WCl6 and SiI4. The reaction proceeds at moderate temperatures in a closed glass vessel. The new compounds W3I12 (W3I8⋅2 I2) and W3I9 (W3I8⋅
- Subjects
IODIDES; TUNGSTEN compounds synthesis; ELECTRONIC structure; CHEMICAL reactions; THERMOLYSIS; CRYSTAL structure
- Publication
Angewandte Chemie International Edition, 2016, Vol 55, Issue 15, p4814
- ISSN
1433-7851
- Publication type
Article
- DOI
10.1002/anie.201509084