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- Title
(E)-1-(1-(Benzofuran-2-yl)ethylidene)-2-(2,4,6-trichlorophenyl)hydrazine.
- Authors
Abdel-Wahab, Bakr F.; Mohamed, Hanan A.; Kariuki, Benson M.; El-Hiti, Gamal A.
- Abstract
The reaction of a mixture of equimolar quantities of 2-acetylbenzofuran and (2,4,6-trichlorophenyl)hydrazine in ethanol containing concentrated hydrochloric acid (0.2 mL; 37%) as a catalyst under reflux for two hours yielded 1-(1-(benzofuran-2-yl)ethylidene)-2-(2,4,6-trichlorophenyl)hydrazine. The crude product was purified by crystallization using dimethylformamide to provide the title heterocycle in a 90% yield. The structure of the new heterocycle was confirmed through X-ray diffraction and spectral analyses.
- Subjects
HYDRAZINE; HYDRAZINES; X-ray diffraction; ETHANOL; HYDROCHLORIC acid; DIMETHYLFORMAMIDE
- Publication
Molbank, 2024, Vol 2024, Issue 1, pM1790
- ISSN
1422-8599
- Publication type
Article
- DOI
10.3390/M1790