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Title
The facile and efficient synthesis of 8-chloroadenosine 3′,5′-cyclic monophosphate by phosphorylative cyclization of 8-chloroadenosine and its characterization by<sup>1</sup>H and<sup>13</sup>C NMR spectroscopy.
Purine nucleosides were chlorinated by the reaction of acyl chloride in DMF with MCPBA under mild conditions with moderate yields. And, satisfactory method for the synthesis of ribonucleoside-3′,5′-cyclic phosphates and its characterization by1H and13C nmr spectroscopy is described.