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- Title
Synergistic effects of hybrid microfibers on mechanical, thermal, and microstructural characterization of nanocomposites.
- Authors
Kahla, Nabil Ben; Raza, Ali; Elhag, Ahmed Babeker; Haider, Hammad
- Abstract
The use of geopolymers (GP) in cementitious composites provides a solution to reduce the significant carbon emissions associated with conventional cement production, thereby advancing environmentally friendly concrete construction practices. The promise of hybrid fiber-reinforced fly ash (FA)-based GP (HFGP) composites that combine microfibers and nanoparticles has not yet been fully comprehended. This research aims to enhance the mechanical and microstructural properties of HFGP blends by varying the proportion of nano calcium carbonate ( n - C a C O 3 ). The production of HFGP involved the use of two types of fibers: 1% carbon fibers and 0.5% basalt fibers. To achieve HFGP blends with a consistent fiber ratio, we incorporated four different levels of n - C a C O 3 , comprising 1%, 2%, 3%, and 4% of the mixture. The analysis of fractured samples encompassed microstructural and mineralogical characterization, which was conducted using scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), and X-ray diffraction (XRD) analysis. The results unveiled that the HFGP blend containing 3% n - C a C O 3 exhibited the highest levels of hardness, compressive strength, toughness modulus, and flexural strength while the use of 2% n - C a C O 3 produced the highest results for fracture toughness and impact strength. SEM analysis illustrated that n - C a C O 3 had a significant positive impact on the microstructure of GP. A considerable rise in hump intensity between 20 and 40 °C ( 2 θ ) was also seen in the XRD examination, indicating that calcium silicate hydrate (CSH) had formed after the primary binder, such as sodium aluminosilicate hydrate (NASH), had been present. The stretching of O–H bonds in water molecules was also seen in the HFGP spectra at 3399, 3436, 3436, and 3438 cm−1. Due to the higher water content in the HFGP network, which may influence the material's strength, these bands were more apparent and larger in specimens with additions of nanoparticles and hybrid fibers.
- Subjects
MICROFIBERS; FOURIER transform infrared spectroscopy; CARBON fibers; CALCIUM silicate hydrate; CEMENT composites; IMPACT strength
- Publication
Environmental Science & Pollution Research, 2024, Vol 31, Issue 17, p25991
- ISSN
0944-1344
- Publication type
Article
- DOI
10.1007/s11356-024-32875-0