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- Title
Visible-Light-Photocatalyzed C5-H Nitration of 8-Aminoquinoline Amides.
- Authors
Liu, Pugen; Qiao, Huijie; Su, Xiaoxue; Bai, Peirong; Yang, Fan
- Abstract
A mild and efficient protocol for visible-light-photocatalyzed C5 nitration of 8-aminoquinoline derivatives was developed utilizing Cu(NO3)2∙3H2O as a nitro source. The reaction proceeded smoothly under very mild conditions, employing Acid Red 94 and a commercial household light bulb as an organic photosensitizer and a light source, respectively, making this synthetic procedure green and easy to operate. Furthermore, most products could be obtained through recrystallization, which enhanced the operational simplicity of this method.
- Subjects
NITRATION; LIGHT sources; RECRYSTALLIZATION (Metallurgy); COPPER; LIGHT bulbs
- Publication
Catalysts (2073-4344), 2024, Vol 14, Issue 4, p263
- ISSN
2073-4344
- Publication type
Article
- DOI
10.3390/catal14040263