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- Title
Anodic fluorination of 4-methoxy-1-naphthol and 4-nitroanisole using EtN · 5 HF in mixed nonaqueous solvent.
- Authors
Saraswat, A.; Sharma, L.; Singh, S.; Siddiqui, I.; Singh, R.
- Abstract
Anodic fluorination of 4-methoxy-1-naphthol and 4-nitroanisole has been investigated in a mixed nonaqueous solvent using EtN · 5 HF as supporting electrolyte as well as fluorine source. In order to avoid the formation of polymer on the anode, pulse electrolysis was carried out without exchanging the electrodes. The proposed procedure ensures excellent yield at room temperature, shortest reaction time, and easy work-up which provide additional advantages in the context of green chemistry. Experimental parameters of the reaction are discussed.
- Subjects
FLUORINATION; METHOXY compounds; NITROANISOLES; NONAQUEOUS solvents; ELECTROLYTES; ANODES; ELECTROLYSIS; SUSTAINABLE chemistry
- Publication
Russian Journal of Organic Chemistry, 2013, Vol 49, Issue 9, p1287
- ISSN
1070-4280
- Publication type
Article
- DOI
10.1134/S107042801309008X