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- Title
New method of synthesis of naphtylthioacetic acids 1-dialkylamides from 4-(1-naphthyl)-1,2,3-thiadiazole.
- Authors
Yekhlef, M.; Petrov, M.; Pevzner, L.
- Abstract
The article presents experiments which synthesized 1-naphthylthioacetic acids dialkylamides using a mixture of ethoxycarbonylhydrazone with thionyl chloride. The synthesis led to the formation of potassium 2-(1-naphthyl)ethynylthiolate with nitrogen release, dialkylamides of naphthylthioacetic acids and tautomers, 2-(1-naphthyl)ethynylthiol. The confirmation of the structure of dithiol is made by nuclear magnetic resonance (NMR) spectroscopy.
- Subjects
ACETIC acid reduction; THIOL synthesis; ETHYNYL compounds; NAPHTHALENE derivatives; AMIDE synthesis
- Publication
Russian Journal of General Chemistry, 2016, Vol 86, Issue 7, p1762
- ISSN
1070-3632
- Publication type
Article
- DOI
10.1134/S1070363216070379