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- Title
Complementing diffraction data with volumetric measurements.
- Authors
Dziubek; Katrusiak
- Abstract
The volumetric measurements in a piston-and-cylinder press have been described as a complementary method for diffraction experiments in a diamond-anvil cell. The measurements can provide precise volume compression data for liquids and solids, including the magnitudes of volume decrement on freezing and solid-solid phase transitions. Details of the experimental setup, its operation, as well as procedures for processing the data and their analysis have been presented for a series of organic compounds. The history of the method has been outlined.
- Subjects
X-ray diffraction; FREEZING; ORGANIC compounds; SOLID-solid interfaces; DATA analysis
- Publication
Zeitschrift für Kristallographie. Crystalline Materials, 2014, Vol 229, Issue 2, p129
- ISSN
2194-4946
- Publication type
Article
- DOI
10.1515/zkri-2013-1677