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- Title
Novel D-glucose and D-mannose based oligomers: synthesis and characterization.
- Authors
Pană, Ana-Maria; Rusnac, Lucian-Mircea; Bandur, Geza; Silion, Mihaela; Deleanu, Călin; Bălan, Mihaela
- Abstract
This paper presents the synthesis and characterization of two oligomers based on monosaccharides (D-glucose and D-mannose). The oligomers were obtained by the polycondensation of two diacids derived from monosaccharides (3- O-benzyl-5,6-(bis(maleyloxy))-1,2-O-isopropylideneglucofuranose and 1-O-benzyl- 5,6-(bis(maleyloxy))-2,3-O-isopropylidenemannofuranose, respectively), with propane-1,3-diol in the presence of p-toluenesulfonic acid. The oligomers were characterized using FTIR and NMR spectroscopy, HPLC-MS and DSC. The copolymerization of the oligomers with 2-hydroxy-propyl acrylate was studied by DSC to evaluate the possibility of obtaining cross-linked copolymers.
- Subjects
GLUCOSE; MANNOSE; OLIGOMERS; MONOSACCHARIDES; POLYCONDENSATION
- Publication
e-Polymers, 2011, p1
- ISSN
1618-7229
- Publication type
Article