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- Title
Crystal structure of K<sub>2</sub>[Mo<sub>3</sub>(PdPPh<sub>3</sub>)S<sub>4</sub>(C<sub>2</sub>O<sub>4</sub>)<sub>3</sub>(H<sub>2</sub>O)<sub>3</sub>]·0.5H<sub>2</sub>O.
- Authors
Gushchin, A. L.; Sokolov, M. N.; Naumov, D. Yu.; Fedin, V. P.
- Abstract
By the reaction of [Mo3S4(C2O4)3(H2O)3]2− with PdCl2 and NH4H2PO2 as a reducing agent, followed by the addition of PPh3, a new oxalate cuboidal cluster complex [Mo3(PdPPh3)S4(C2O4)3(H2O)3]2− is obtained. It was isolated and structurally characterized as K2[Mo3(PdPPh3)S4(C2O4)3(H2O)3]·0.5H2O.
- Subjects
CHEMICAL structure; CHEMICAL reactions; MOLYBDENUM; PALLADIUM; X-rays; MICROCLUSTERS
- Publication
Journal of Structural Chemistry, 2008, Vol 49, Issue 4, p748
- ISSN
0022-4766
- Publication type
Article
- DOI
10.1007/s10947-008-0105-5