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- Title
Heterocyclizations of 1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide.
- Authors
Savitskii, P. V.; Vas'kevich, R. I.; Zborovskii, Yu. L.; Staninets, V. I.; But, S. A.; Chernega, A. N.
- Abstract
1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide reacted with methyl iodide in the presence of sodium acetate in boiling ethanol to give 2,2′-dithiobis[ N-(5-methylsulfanyl-4-phenyl-4 H-1,2,4-triazol-3-yl)-benzenamine]. The reaction of the title compound with dimethyl acetylenedicarboxylate in dioxane led to the formation of methyl 3-(benzothiazol-2-yl)-2-(2-methoxy-2-oxoethyl)-2,3-dihydro-1,3,4-thiadiazole-2-carboxylate.
- Subjects
SODIUM acetate; ACETATES; ALCOHOL; PHENYL compounds; BIFONAZOLE; ETHANES; DIOXANE; THIADIAZOLES
- Publication
Russian Journal of Organic Chemistry, 2008, Vol 44, Issue 3, p402
- ISSN
1070-4280
- Publication type
Article
- DOI
10.1134/S1070428008030159