We found a match
Your institution may have access to this item. Find your institution then sign in to continue.
- Title
Quantitative Online NMR Spectroscopy in a Nutshell.
- Authors
Zientek, Nicolai; Meyer, Klas; Kern, Simon; Maiwald, Michael
- Abstract
Online NMR spectroscopy is an excellent tool to study complex reacting multicomponent mixtures and gain process insight and understanding. For online studies under process conditions, flow NMR probes can be used in a wide range of temperature and pressure. This paper compiles the most important aspects towards quantitative process NMR spectroscopy in complex multicomponent mixtures and provides examples. After NMR spectroscopy is introduced as an online method and for technical samples without sample preparation in deuterated solvents, influences of the residence time distribution, pre-magnetization, and cell design are discussed. NMR acquisition and processing parameters as well as data preparation methods are presented and the most practical data analysis strategies are introduced.
- Subjects
NUCULIDAE; NUCLEAR magnetic resonance spectroscopy; MAGNETIZATION; DATA analysis; OLAP technology
- Publication
Chemie Ingenieur Technik (CIT), 2016, Vol 88, Issue 6, p698
- ISSN
0009-286X
- Publication type
Article
- DOI
10.1002/cite.201500120