We found a match
Your institution may have access to this item. Find your institution then sign in to continue.
- Title
Multicomponent Synthesis of 1,3-Bis[(alkylsulfanyl)methyl]-1,3,5-triazinan-2-ones.
- Authors
Baeva, L. A.; Biktasheva, L. F.; Nugumanov, T. R.; Fatykhov, A. A.
- Abstract
Previously unknown 5-alkyl-1,3-bis[(alkylsulfanyl)methyl]-1,3,5-triazinan-2-ones have been syn-thesized by three-component condensation of available N,N′-bis[(alkylsulfanyl)methyl]ureas with formaldehyde and primary amines in ethanol in the presence of sodium hydroxide or triethylamine. A one-pot four-component procedure has been proposed for the synthesis of the title compounds via successive thiomethylation of urea with a mixture of formaldehyde and alkanethiol and cycloaminomethylation of intermediate N,N′-bis[(alkyl-sulfanyl)methyl]ureas with formaldehyde and alkylamine.
- Subjects
UREA-formaldehyde resins; SODIUM hydroxide; MANNICH reaction; TRIETHYLAMINE
- Publication
Russian Journal of Organic Chemistry, 2021, Vol 57, Issue 12, p1948
- ISSN
1070-4280
- Publication type
Article
- DOI
10.1134/S1070428021120071