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- Title
New representatives of nitroamine-containing 1,2,4-triazoles: Synthesis and structure.
- Authors
Efimova, T.; Ozerova, O.; Novikova, T.; Belik, I.; Berestovitskaya, V.
- Abstract
The interaction of 1-methyl-1-nitroso-2-nitroguanidine with carboxylic acid hydrazides results in formation of N-(2-nitroguanidino)amides that easily give 3(5)-nitroamino-5(3)-alkyl(aryl)-1,2,4-triazoles under refluxing in aqueous alkaline medium. We have developed a one-pot method to prepare such heterocyclic structures; the synthesis of one of the sample compound has given an example of the method applicability. The compounds structures have been confirmed by UV, IR, H, and C-{H} NMR spectroscopy.
- Subjects
NITROGUANIDINE; CARBOXYLIC acids; NITROAMINES; HYDRAZIDES; TRIAZOLES; NUCLEAR magnetic resonance spectroscopy
- Publication
Russian Journal of General Chemistry, 2013, Vol 83, Issue 9, p1779
- ISSN
1070-3632
- Publication type
Article
- DOI
10.1134/S1070363213090259