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- Title
A Low Temperature Synthetic Route to Nanocrystalline TiN.
- Authors
Pei-jun Cai; Gong-zhen Li; Chong Shi; Jun-hao Huo; Li-hua Liu
- Abstract
A simple chemical synthetic route has been developed to prepare nanocrystalline titanium nitride (TiN) in an autoclave, by the reaction of metallic Ti with NaNH2 at low temperature of 500-600 °C. The samples were characterized by X-ray powder diffraction, transmission electron microscopy, and X-ray photoelectron spectra. The possible reaction mechanism of this process is also discussed. This method may be extended to the synthesis of other metal nitrides.
- Subjects
TITANIUM nitride; NANOCRYSTALS; AUTOCLAVES; TRANSMISSION electron microscopy; X-ray diffraction; LOW temperatures
- Publication
South African Journal of Chemistry, 2011, Vol 64, p57
- ISSN
0379-4350
- Publication type
Article