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- Title
Direct Synthesis of Nitriles from Aldehydes and Hydroxylamine Hydrochloride Catalyzed by a HAP@AEPH<sub>2</sub>-SO<sub>3</sub>H Nanocatalyst.
- Authors
Masjed, Samane Memar; Akhlaghinia, Batool; Zarghani, Monireh; Razavi, Nasrin
- Abstract
We describe an efficient method for the direct preparation of nitriles from aldehydes and hydroxylamine hydrochloride catalyzed by sulfonated nanohydroxyapatite functionalized by 2-aminoethyl dihydrogen phosphate (HAP@AEPH2- SO3H) as an eco-friendly and recyclable solid acid nanocatalyst. In this protocol the use of a solid acid nanocatalyst provides a green, useful, and rapid method for the preparation of nitriles in excellent yields. In addition, the notable feature of this methodolgy is that the synthesized nanocatalyst can be recovered and reused five times without any noticeable loss of efficiency.
- Subjects
NITRILE synthesis; ALDEHYDES; HYDROXYLAMINE hydrochloride
- Publication
Australian Journal of Chemistry, 2017, Vol 70, Issue 1, p33
- ISSN
0004-9425
- Publication type
Article
- DOI
10.1071/CH16126