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- Title
Bis-heterocycles. Part I: tetrahydro-5,5′- bi(1,2,4-triazin-6-ones).
- Authors
Mohammad, Hanan H.; El-Abadelah, Mustafa M.; Sabri, Salim S.; Awwadi, Firas F.; Voelter, Wolfgang
- Abstract
Selected sets of tetrahydro-5,5′-bi(1,2,4-triazines) (1–3) appended with acetyl, benzoyl, and ester moieties at C-3 position and N-1 (p-substituted)phenyl ring have been prepared and characterized by spectral (IR, NMR, MS) data and X-ray diffraction for compound 3a. Their synthesis was achieved in high yield via the reaction of diethyl aminomalonate with various N-(aryl)hydrazonoyl chlorides in the presence of triethylamine.
- Subjects
HETEROCYCLIC compounds; TRIAZINES; NUCLEAR magnetic resonance spectroscopy; X-ray diffraction; TRIETHYLAMINE
- Publication
Zeitschrift für Naturforschung B: A Journal of Chemical Sciences, 2018, Vol 73, Issue 12, p965
- ISSN
0932-0776
- Publication type
Article
- DOI
10.1515/znb-2018-0148