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- Title
Synthesis and Structure Determination of 2-Cyano-3-(1-phenyl-3-(thiophen-2-yl)-1 H -pyrazol-4-yl)acrylamide.
- Authors
Kariuki, Benson M.; Abdel-Wahab, Bakr F.; Mohamed, Hanan A.; El-Hiti, Gamal A.
- Abstract
2-Cyano-3-(1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-4-yl)acrylamide (3) was synthesized in 90% yield from condensation of equimolar equivalents of 1-phenyl-3-(thiophen-2-yl)-1H-pyrazole-4-carbaldehyde (1) and 2-cyanoacetamide (2) in boiling ethanol under basic condition for 45 min. The structure of 3 was determined using NMR spectroscopy and single crystal X-ray diffraction.
- Subjects
NUCLEAR magnetic resonance spectroscopy; SINGLE crystals; X-ray diffraction; CONDENSATION
- Publication
Molbank, 2022, Vol 2022, Issue 2, pM1372
- ISSN
1422-8599
- Publication type
Article
- DOI
10.3390/M1372