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- Title
Chlorination of geminal bis(alkoxy- NNO-azoxy) compounds with sodium hypochlorite.
- Authors
Zyuzin, I.
- Abstract
Chlorination of geminal bis(alkoxy- NNO-azoxy) compounds with sodium hypochlorite involves the central carbon atom and gives 1,1-bis(alkoxy- NNO-azoxy)-1-chloroalkanes with high yield. Dichlorobis-(methoxy- NNO-azoxy)methane oxidizes sodium iodide to elemental iodine. The signal from the central carbon atom in the C NMR spectra of bis(alkoxy- NNO-azoxy)dichloromethanes is broadened and displaced downfield relative to those of the initial compounds.
- Subjects
AZOXY compounds; CHLORINATION; AZO compound synthesis; NITROGEN compound synthesis; SODIUM hypochlorite
- Publication
Russian Journal of Organic Chemistry, 2014, Vol 50, Issue 9, p1252
- ISSN
1070-4280
- Publication type
Article
- DOI
10.1134/S1070428014090036