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- Title
Microwave-assisted solvent-free synthesis and spectral and structural characterization of cyclotriphosphazene hexakis(o-tolylamide).
- Authors
Hakimi, Mohammad; Rezaei, Homeyra; Moeini, Keyvan; Raissi, Heidar; Eigner, Vaclav; Dušek, Michal
- Abstract
A new cyclotriphosphazene, 2,2,4,4,6,6-hexakis (o-tolylamono)-1,3,5,2λ5,4λ5,6λ5-triazatriphosphinine (MPAP), was prepared using microwave irradiation and identified by elemental analysis, FT-IR, Raman, 31P NMR spectroscopy, and single-crystal X-ray diffraction. In the crystal, in addition to hydrogen bonds, the network is further stabilized by inter- and intramolecular π–π stacking interactions between aromatic rings.
- Subjects
SOLVENTS; CYCLOTRIPHOSPHAZENES; AMIDES; FOURIER transform infrared spectroscopy; SINGLE crystals; NUCLEAR magnetic resonance spectroscopy
- Publication
Zeitschrift für Naturforschung B: A Journal of Chemical Sciences, 2018, Vol 73, Issue 12, p999
- ISSN
0932-0776
- Publication type
Article
- DOI
10.1515/znb-2018-0136