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- Title
Bis(4-nitrophenyl)phosphorylazide as a reagent for direct azidation of polyfunctional derivatives of pyrimidin-4(3 Н)-one.
- Authors
Novakov, I.; Babushkin, A.; Brunilina, L.; Navrotskii, M.; Orlinson, B.; Robinovich, M.; Yablokov, A.
- Abstract
The application of bis-(4-nitrophenyl)phosphorylazide-1,8-diazabicyclo[5.4.0]undec-7-ene system for direct transformation of polyfunctional derivatives of pyrimidin-4(3 H)-one in the corresponding 4-azidopyrimidines has been suggested for the first time. Using this system, novel 4-azido-6-(2,6-dihalo-α-methoxybenzyl)-5-methyl-2-(nitroamino)pyrimidines have been obtained in good yield under mild conditions.
- Subjects
PYRIMIDINES; CHEMICAL reagents; AZIDATION; NITROPHENYL compounds; AZIDO group
- Publication
Russian Journal of General Chemistry, 2017, Vol 87, Issue 2, p219
- ISSN
1070-3632
- Publication type
Article
- DOI
10.1134/S1070363217020116