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- Title
Direct Synthesis of Carbamoyl Fluorides by CO<sub>2</sub> Deoxyfluorination.
- Authors
Onida, Killian; Tlili, Anis
- Abstract
Herein, a new concept for the direct synthesis of carbamoyl fluoride derivatives is disclosed. The developed method makes use of CO2 as an inexpensive and abundant C1 source; a variety of amines were successfully converted in the presence of a deoxyfluorinating reagent. The corresponding products were often obtained in excellent yields under mild reaction conditions (1 atm and room temperature). The reaction was easily scaled up, demonstrating the efficiency of the developed process.
- Subjects
AMINES; FLUORITE; TEMPERATURE
- Publication
Angewandte Chemie, 2019, Vol 131, Issue 36, p12675
- ISSN
0044-8249
- Publication type
Article
- DOI
10.1002/ange.201907354