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- Title
(E)-1-(4-Methoxyphenyl)-5-methyl-4-(1-phenyl-4-((2-(2,4,6-trichlorophenyl)hydrazineylidene)methyl)-1 H -pyrazol-3-yl)-1 H -1,2,3-triazole.
- Authors
Abdel-Wahab, Bakr F.; Mohamed, Hanan A.; Kariuki, Benson M.; El-Hiti, Gamal A.
- Abstract
The reaction of equimolar quantities of 3-(1-(4-methoxyphenyl)-5-methyl-1H-1,2,3-triazol-4-yl)-1-phenyl-1H-pyrazole-4-carbaldehyde and (2,4,6-trichlorophenyl)hydrazine in ethanol containing concentrated hydrochloric acid (0.2 mL; 37%) as a catalyst under reflux for 2 h yielded 1-(1-(benzofuran-2-yl)ethylidene)-2-(2,4,6-trichlorophenyl)hydrazine. The crude produced was purified by crystallization using dimethylformamide to provide the title heterocycle in a 95% yield. The structure of the newly synthesized heterocycle was confirmed through X-ray diffraction and spectral analyses.
- Subjects
HYDRAZINE; X-ray diffraction; HYDROCHLORIC acid; ETHANOL; HYDRAZINES; DIMETHYLFORMAMIDE
- Publication
Molbank, 2024, Vol 2024, Issue 2, pM1798
- ISSN
1422-8599
- Publication type
Article
- DOI
10.3390/M1798