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Title
A Catalyst-Free, One-Pot Three-Component Aminomethylation of α-Substituted Nitroacetates: Theoretical and Experimental Studies into the Rate-Accelerating Effects of the Solvent Methanol.
3, 2, 1 go! An unprecedented one ‐ pot, catalyst ‐ free, three ‐ component aminomethylation of α ‐ substituted nitroacetates, formalin, and amines has been reported, thereby enabling the highly efficient synthesis of α,β ‐ diamino acid precursors with great structural diversity.