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- Title
A simplified synthesis of 2-acetyl-1,4,5,8-tetramethoxynaphthalene and its selective demethylation product.
- Authors
Dong, J.; Zhang, Q.; Meng, Q.; Huang, G.; Zhou, W.; Li, Shaoshun
- Abstract
Based on the Friedel-Crafts acylation reaction, a one-step synthesis of 2-acetyl-1,4,5,8-tetramethoxynaphthalene and its selective demethylation product was carried out under various reaction conditions. The product and yield of the reaction were highly catalyst and solvent dependent. The developed method is characterized by short process time, low cost, mild conditions, simple work-out, high yield, and low chemical waste.
- Subjects
ACETYL compounds; DEMETHYLATION; FRIEDEL-Crafts reaction; CHEMICAL yield; LEWIS acids
- Publication
Russian Journal of General Chemistry, 2016, Vol 86, Issue 12, p2877
- ISSN
1070-3632
- Publication type
Article
- DOI
10.1134/S1070363216120549