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- Title
Synthesis and crystal structure of (R)-(-)- N-dichloroacetyl-3-ethyl-1-oxa-4-aza-spiro-4.5-decane.
- Authors
Zhao, Li-Xia; Fu, Ying; Ye, Fei; Gao, Shuang
- Abstract
The title compound, (R)-(-)- N-dichloroacetyl-3-ethyl-1-oxa-4-aza-spiro-4.5-decane 3 was synthesized by a sequential procedure involving condensation of (R)-2-amino-butanol with cyclohexanone and acylation of the resultant intermediate spiro compound with dichloroacetyl chloride. The X-ray structure determination confirmed the structure and the product was further characterized by IR, 1H-NMR, and 13C-NMR spectroscopy, mass spectrometry, and elemental analysis.
- Subjects
AMINO acids; BUTANOL; CYCLOHEXANONES; ACYLATION; ORGANIC synthesis; SPECTRUM analysis
- Publication
Heterocyclic Communications, 2011, Vol 17, Issue 1/2, p53
- ISSN
0793-0283
- Publication type
Article
- DOI
10.1515/HC.2011.003