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- Title
Synthesis and crystal structure of mixed-ligand Cu(II) complex of N-(1-phenyl-3-methyl-4-benzylidene- 5-pyrazolone) p-nitrobezoylhydrazide and pyridine.
- Authors
Zhang, Li; Liu, Lang; Liu, Guang-Fei; Xu, Guan-Cheng; Jia, Dian-Zeng; Lang, Jian-Ping
- Abstract
A new mixed-ligand copper(II) complex, [Cu(PMBP-PNH)Py], (PMBP-PNH = N-(1-phenyl-3-methyl-4-benzylidene-5-pyrazolone) p-nitrobezoylhydrazide; Py = pyridine), has been synthesized by solvothermal method and characterized by elemental analysis, IR spectrum, thermal analysis and single crystal X-ray diffraction: monoclinic, space group Cc with a = 6.0422(8) Å, b = 22.796(3) Å, c = 18.353(3) Å, β = 93.199(3)∘, Mr = 582.08, V = 2524.0(6) Å3, Z = 4. The copper(II) ion in the title complex is in a slightly distorted square-planar arrangement of the ONO donor atoms of primary ligand PMBP-PNH and one N-donor atom in the secondary ligand pyridine.
- Publication
Journal of Chemical Crystallography, 2005, Vol 35, Issue 8, p583
- ISSN
1074-1542
- Publication type
Article
- DOI
10.1007/s10870-005-2869-1