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- Title
Synthesis and properties of novel magnetic nanoparticles grafted with nitropyridine-substituted calix[4]arene derivative as Cr<sup>6+</sup> extractant.
- Authors
SAYIN, Serkan; DOĞGAN, Vildan
- Abstract
A new calix[4]arene derivative, 3, which functionalized at the lower rim with 2-(2-aminoethyl amino)-5-nitropyridine, was synthesized and characterized by a combination of FTIR, 1H NMR, 13C NMR, and elemental analysis. Then the calix[4]arene 3 was grafted onto [3-(2,3-epoxypropoxy)propyl]trimethoxysilane-modified Fe3O4 - nanoparticles (EPPTMS-MN) to produce new calixarene-adorned magnetic nanoparticles (MN-DiNoPy-Calix (4)). The structure of the calixarene-adorned magnetic nanoparticles 4 was determined by a combination of FTIR, TEM, and elemental analysis. Moreover, a study regarding the removal of toxic HCr2O-7 anion from aqueous solution was also carried out with the calixarene-adorned magnetic nanoparticles in solid-liquid extraction studies.
- Subjects
CHEMICAL synthesis; MAGNETIC nanoparticles; CALIXARENE derivatives; PYRIDINE; NUCLEAR magnetic resonance; FOURIER transform infrared spectroscopy
- Publication
Turkish Journal of Chemistry, 2015, Vol 39, Issue 1, p130
- ISSN
1300-0527
- Publication type
Article
- DOI
10.3906/kim-1405-69